| 大薊 |
 |
|
|
|
|
| 蒙花苷(Linarin)的結構 |
 |
| 蒙花苷(Linarin)的1H NMR圖譜 |
|
| 蒙花苷(Linarin)的13C NMR圖譜 |
 13C
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| 蒙花苷(Linarin)的ESI-MS圖譜 |
 |
| 蒙花苷(Linarin)的FTIR圖譜 |
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| 蒙花苷(Linarin)的分子式、分子量與熔點 |
白色固體；分子式：C28H32O14 Mol. Wt.: 592.54 mp: 258–260 °C |
| 蒙花苷(Linarin)的氫、碳化學位移 |
蒙花苷(Linarin)的氫、碳化學位移(DMSO-d6)a
|
position
|
dH (600 MHz)
|
dC (150 MHz)
|
|
1
|
-
|
-
|
|
2
|
-
|
163.9
|
|
3
|
6.96 (s)
|
103.8
|
|
4
|
-
|
182.0
|
|
5
|
-
|
161.1
|
|
6
|
6.45 (d, 2.0)
|
99.6
|
|
7
|
-
|
163.0
|
|
8
|
6.79 (d, 2.0)
|
94.8
|
|
9
|
-
|
157.0
|
|
10
|
-
|
105.5
|
|
1’
|
-
|
122.7
|
|
2’
|
8.06 (d, 8.9)
|
128.5
|
|
3’
|
7.15 (d, 8.9)
|
114.7
|
|
4’
|
-
|
162.4
|
|
5’
|
7.15 (d, 8.9)
|
114.7
|
|
6’
|
8.06 (d, 8.9)
|
128.5
|
|
1’’
|
5.06 (d, 7.1)
|
99.9
|
|
2’’
|
3.31 (m)
|
73.1
|
|
3’’
|
3.31 (m)
|
76.2
|
|
4’’
|
3.16 (m)
|
68.3
|
|
5’’
|
3.61 (m)
|
75.7
|
|
6’’
|
3.46 (m); 3.86 (m)
|
66.1
|
|
1’’’
|
4.55 (d, 1.0)
|
100.5
|
|
2’’’
|
3.05 (m)
|
70.3
|
|
3’’’
|
3.45 (m)
|
70.7
|
|
4’’’
|
3.13 (m)
|
72.0
|
|
5’’’
|
3.39 (m)
|
69.5
|
|
6’’’
|
1.08 (d, 6.2)
|
17.8
|
|
4’-OMe
|
3.86 (s)
|
55.6
|
|
a(Multiplicity, J in Hz) in ppm.
|
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