|
position
|
|
dH (600 MHz)
|
|
dC (150 MHz)
|
|
|
1
|
|
|
|
145.11
|
|
|
2
|
|
|
|
151.95
|
|
|
3
|
|
6.61 (s)
|
|
111.23
|
|
|
4
|
|
|
|
128.70
|
|
|
5
|
|
a: 3.15 (m)
b: 2.66 (dd, 16.2, 1.8)
|
|
29.24
|
|
|
6
|
|
a: 3.20 (m)
b: 2.49 (td, 12.0, 4.2)
|
|
53.28
|
|
|
7
|
|
3.00 (m)
|
|
62.32
|
|
|
8
|
|
a: 2.59 (t, 13.8)
b: 3.07 (dd, 13.8, 4.2)
|
|
35.12
|
|
|
9
|
|
|
|
136.47
|
|
|
10
|
|
7.24 (br d, 6.6)
|
|
127.83
|
|
|
11
|
|
7.21 (td, 7.2, 1.2)
|
|
127.28
|
|
|
12
|
|
7.29 (m)
|
|
126.97
|
|
|
13
|
|
8.34 (br d, 7.8)
|
|
128.30
|
|
|
14
|
|
|
|
132.13
|
|
|
15
|
|
|
|
126.86
|
|
|
16
|
|
|
|
127.99
|
|
|
17
|
|
3.64 (s)
|
|
60.21
|
|
|
18
|
|
3.87 (s)
|
|
55.83
|
|
|
19
|
|
2.53 (s)
|
|
44.00
|
|
a(Multiplicity, J in Hz) in ppm. |
