川續斷皂苷VI (Akebia saponin D)氫、碳化學位移
川續斷皂苷VI (Akebia saponin D)氫、碳化學位移(CD3OD)a
|
position
|
dH (600 MHz)
|
dC (150 MHz)
|
|
1
|
0.93, 1.72
|
39.6
|
|
2
|
1.76, 1.89
|
26.3
|
|
3
|
3.61
|
83.3
|
|
4
|
-
|
43.9
|
|
5
|
1.22
|
48.6
|
|
6
|
1.37, 1.45
|
18.9
|
|
7
|
1.45
|
34.9
|
|
8
|
-
|
40.7
|
|
9
|
1.35
|
48.2
|
|
10
|
-
|
37.7
|
|
11
|
1.06, 1.85
|
24.1
|
|
12
|
5.24 (br, s)
|
123.8
|
|
13
|
-
|
145.0
|
|
14
|
-
|
42.6
|
|
15
|
0.90, 1.27
|
28.9
|
|
16
|
1.68, 1.88
|
24.6
|
|
17
|
-
|
48.1
|
|
18
|
2.86 (dd, 3.5, 9.6)
|
43.0
|
|
19
|
1.08, 1.25
|
47.3
|
|
20
|
-
|
31.6
|
|
21
|
1.25, 1.55
|
33.4
|
|
22
|
1.27, 1.58
|
33.2
|
|
23
|
3.34, 3.51
|
64.6
|
|
24
|
0.70 (s)
|
13.4
|
|
25
|
0.98 (s)
|
16.6
|
|
26
|
0.79 (s)
|
17.9
|
|
27
|
1.16 (s)
|
26.4
|
|
28
|
-
|
178.1
|
|
29
|
0.90 (s)
|
33.5
|
|
30
|
0.93 (s)
|
24.1
|
|
Glc-1
|
|
|
|
1
|
5.33 (d, 8.4)
|
95.8
|
|
2
|
3.41
|
75.1
|
|
3
|
3.36
|
78.0
|
|
4
|
3.49
|
71.0
|
|
5
|
3.44
|
77.8
|
|
6
|
2.86, 4.12 (dd, 1.4, 11.6)
|
69.5
|
|
Glc-2
|
|
|
|
1
|
4.36 (d, 9.6)
|
104.7
|
|
2
|
3.36
|
73.9
|
|
3
|
3.40
|
78.2
|
|
4
|
3.32
|
71.6
|
|
5
|
3.48
|
78.1
|
|
6
|
3.61 (m), 3.85 (m)
|
62.7
|
|
Ara-1
|
|
|
|
1
|
4.30 (7.2)
|
106.4
|
|
2
|
3.66
|
73.0
|
|
3
|
3.60
|
74.5
|
|
4
|
3.76
|
69.8
|
|
5
|
3.51 (m), 3.84 (m)
|
66.8
|
|
