穗花杉雙黃酮(Amentoflavone)的氫、碳化學位移(DMSO-d6)a
position
|
|
H (600 MHz)
|
|
C
|
|
position
|
|
H (600 MHz)
|
|
C
|
|
2
|
|
|
|
163.8
|
|
2’
|
|
|
|
163.7
|
|
3
|
|
6.83 (s)
|
|
102.9
|
|
3’
|
|
6.79 (s)
|
|
102.6
|
|
4
|
|
|
|
181.7
|
|
4’
|
|
|
|
182.1
|
|
4a
|
|
|
|
103.7
|
|
4a’
|
|
|
|
103.6
|
|
5
|
|
|
|
161.4
|
|
5’
|
|
|
|
160.5
|
|
6
|
|
6.18 (d, 1.8)
|
|
98.8
|
|
6’
|
|
6.39 (s)
|
|
98.6
|
|
7
|
|
|
|
164.1
|
|
7’
|
|
|
|
162.0
|
|
8
|
|
6.45 (d, 1.8)
|
|
94.0
|
|
8’
|
|
|
|
104.0
|
|
8a
|
|
|
|
157.3
|
|
8a’
|
|
|
|
154.5
|
|
9
|
|
|
|
120.9
|
|
9’
|
|
|
|
121.4
|
|
10
|
|
7.99 (d, 2.4)
|
|
131.4
|
|
10’
|
|
7.56 (d, 8.4)
|
|
128.2
|
|
11
|
|
|
|
120.0
|
|
11’
|
|
6.70 (d, 8.4)
|
|
115.7
|
|
12
|
|
|
|
159.9
|
|
12’
|
|
|
|
161.0
|
|
13
|
|
7.13 (d, 9.6)
|
|
116.2
|
|
13’
|
|
6.70 (d, 8.4)
|
|
115.7
|
|
14
|
|
8.00 (d, 9.6, 2.4)
|
|
127.8
|
|
14’
|
|
7.56 (d, 8.4)
|
|
128.2
|
|
5-OH
|
|
13.0 (s)
|
|
|
|
5’-OH
|
|
13.1 (s)
|
|
|
|
7-OH
|
|
10.8 (s)
|
|
|
|
7’-OH
|
|
|
|
|
|
12-OH
|
|
|
|
|
|
12’-OH
|
|
10.2 (s)
|
|
|
|
a(Multiplicity, J in Hz) in ppm. |