諾卡酮(Nootkatone)的氫、碳化學位移(CDCl3)a
|
position
|
|
dH (600 MHz)
|
|
dC (150 MHz)
|
|
|
1
|
|
1.98 (m)
|
|
40.4
|
|
|
2
|
|
2.20 (ddd, 0.6, 4.5, 17.4),
2.25 (br d, 13.8)
|
|
42.0
|
|
|
3
|
|
|
|
199.8
|
|
|
4
|
|
5.74 (s)
|
|
124.6
|
|
|
5
|
|
|
|
170.7
|
|
|
6
|
|
2.34 (m), 2.49 (m)
|
|
33.0
|
|
|
7
|
|
1.32 (m), 1.88 (m)
|
|
31.6
|
|
|
8
|
|
2.29 (m)
|
|
40.3
|
|
|
9
|
|
1.11 (m), 1.94 (m)
|
|
43.9
|
|
|
10
|
|
|
|
39.3
|
|
|
11
|
|
|
|
149.0
|
|
|
12
|
|
|
|
109.2
|
|
|
13
|
|
1.71 (s)
|
|
20.8
|
|
|
14
|
|
0.94 (d, 7.2)
|
|
14.9
|
|
|
15
|
|
1.09 (s)
|
|
16.8
|
|
a(Multiplicity, J in Hz) in ppm. |
